Information card for entry 7010960

Structure parameters

• Formula: C23.5 H28 Cl3 N2 O V
• Calculated formula: C23.5 H28.06 Cl3 N2 O V
• Title of publication: Synthesis of α-diimine V(iii) complexes and their role as ethylene polymerisation catalysts
• Authors of publication: Milione, Stefano; Cavallo, Gabriella; Tedesco, Consiglia; Grassi, Alfonso
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 1839
• a: 11.024 ± 0.009 Å
• b: 16.299 ± 0.004 Å
• c: 13.722 ± 0.003 Å
• α: 90°
• β: 90.47 ± 0.05°
• γ: 90°
• Cell volume: 2465 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2047
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.1233
• Weighted residual factors for all reflections included in the refinement: 0.2192
• Goodness-of-fit parameter for all reflections included in the refinement: 0.933
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No