Information card for entry 7010976

Structure parameters

• Chemical name: Ag2(tripod)I2.3DMSO
• Formula: C47 H57 Ag2 I2 O3 P3 S3
• Calculated formula: C47 H57 Ag2 I2 O3 P3 S3
• Title of publication: Comparative structural studies on silver(I) complexes with tripodal polyphosphines. Crystallographic characterisation of the first infinite chain structures in 2 ∶ 1 adducts of silver(I) halides with 1,1,1-tris(diphenylphosphinomethyl)ethane
• Authors of publication: José A. Montes; Susana Rodríguez; Damián Fernández; M. Inés García-Seijo; Robert O. Gould; M. Esther García-Fernández
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1110 - 1118
• a: 13.926 ± 0.004 Å
• b: 19.209 ± 0.005 Å
• c: 19.642 ± 0.005 Å
• α: 90°
• β: 98.19 ± 0.005°
• γ: 90°
• Cell volume: 5201 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2818
• Residual factor for significantly intense reflections: 0.0889
• Weighted residual factors for significantly intense reflections: 0.2137
• Weighted residual factors for all reflections included in the refinement: 0.3008
• Goodness-of-fit parameter for all reflections included in the refinement: 0.888
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No