Information card for entry 7010983

Structure parameters

• Formula: C36 H42.5 Al N1.5 O P
• Calculated formula: C36 H41 Al N1.5 O P
• Title of publication: Synthesis and characterisation of neutral and cationic alkyl aluminium complexes bearing N,O-Schiff base chelates with pendant donor arms
• Authors of publication: Paul A. Cameron; Vernon C. Gibson; Carl Redshaw; John A. Segal; Andrew J. P. White; David J. Williams
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 415 - 422
• a: 15.3292 ± 0.0011 Å
• b: 13.3657 ± 0.0008 Å
• c: 17.5748 ± 0.0008 Å
• α: 90°
• β: 108.813 ± 0.005°
• γ: 90°
• Cell volume: 3408.5 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1164
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for all reflections: 0.2026
• Weighted residual factors for significantly intense reflections: 0.1669
• Goodness-of-fit parameter for all reflections: 1.024
• Goodness-of-fit parameter for significantly intense reflections: 1.108
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No