Information card for entry 7010993

Structure parameters

• Formula: C28 H64 Mo3 O30 Pd S4 Se4
• Calculated formula: C28 H28 Mo3 O30 Pd S4 Se4
• Title of publication: Formation (and properties) of palladium derivatives of [Mo3Q4(H2O)9]4+: absence of similar derivatives of [W3Q4(H2O)9]4+ (Q = S, Se)
• Authors of publication: Vladimir P. Fedin; Mi-Sook Seo; David M. Saysell; Danil N. Dybtsev; Mark R. J. Elsegood; William Clegg; A. Geoffrey Sykes
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 2
• Pages of publication: 138 - 143
• a: 11.6971 ± 0.0011 Å
• b: 14.9372 ± 0.0015 Å
• c: 16.4307 ± 0.0016 Å
• α: 77.38 ± 0.002°
• β: 84.506 ± 0.003°
• γ: 82.822 ± 0.002°
• Cell volume: 2772.5 ± 0.5 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0981
• Weighted residual factors for all reflections included in the refinement: 0.1027
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No