Information card for entry 7011004

Structure parameters

• Formula: C38.5 H54 Cl3 F6 Fe N4 Sb
• Calculated formula: C38.5 H46 Cl3 F6 Fe N4 Sb
• Title of publication: Cationic 2,6-bis(imino)pyridine iron and cobalt complexes: synthesis, structures, ethylene polymerisation and ethylene/polar monomer co-polymerisation studies
• Authors of publication: George J. P. Britovsek; Vernon C. Gibson; Stefan K. Spitzmesser; Kilian P. Tellmann; Andrew J. P. White; David J. Williams
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1159 - 1171
• a: 25.925 ± 0.002 Å
• b: 10.0628 ± 0.0005 Å
• c: 36.759 ± 0.003 Å
• α: 90°
• β: 92.553 ± 0.007°
• γ: 90°
• Cell volume: 9580.1 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1528
• Residual factor for significantly intense reflections: 0.0809
• Weighted residual factors for all reflections: 0.2609
• Weighted residual factors for significantly intense reflections: 0.1896
• Goodness-of-fit parameter for all reflections: 1.025
• Goodness-of-fit parameter for significantly intense reflections: 1.152
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No