#------------------------------------------------------------------------------
#$Date: 2025-08-21 13:21:36 +0200 (Thu 21 de Aug de 2025) $
#$Revision: 301847 $
#$URL: svn://www.crystallography.net/cod/cif/7/01/10/7011050.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7011050
loop_
_publ_author_name
'Alexandra M. Z. Slawin'
'Matthew Wainwright'
'J. Derek Woollins'
_publ_section_title
;
 The preparation and coordination chemistry of phosphorus(III)
 derivatives of dialkyl hydrazines
;
_journal_issue                   4
_journal_name_full               'J. Chem. Soc., Dalton Trans.'
_journal_page_first              513
_journal_page_last               519
_journal_paper_doi               10.1039/b107072j
_journal_year                    2002
_chemical_formula_moiety         'C30 H34 Cl2 N2 O4 P2 Pt.0.5[C H2 Cl2]'
_chemical_formula_sum            'C30.5 H35 Cl3 N2 O4 P2 Pt'
_chemical_formula_weight         856.98
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                96.5460(10)
_cell_angle_beta                 99.1120(10)
_cell_angle_gamma                106.8710(10)
_cell_formula_units_Z            2
_cell_length_a                   10.2861(2)
_cell_length_b                   11.91490(10)
_cell_length_c                   15.9825(2)
_cell_measurement_reflns_used    119
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      168
_cell_measurement_theta_min      12
_cell_volume                     1824.11(5)
_computing_cell_refinement       SMART/SAINT
_computing_data_collection       SMART
_computing_data_reduction        SAINT
_computing_molecular_graphics    SHELXTL
_computing_publication_material  SHELXTL
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_detector_area_resol_mean 0.9
_diffrn_measured_fraction_theta_full 0.980
_diffrn_measured_fraction_theta_max 0.980
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0160
_diffrn_reflns_av_sigmaI/netI    0.0364
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            7820
_diffrn_reflns_theta_full        23.23
_diffrn_reflns_theta_max         23.23
_diffrn_reflns_theta_min         2.25
_exptl_absorpt_coefficient_mu    4.188
_exptl_absorpt_correction_T_max  1.000000
_exptl_absorpt_correction_T_min  0.656461
_exptl_absorpt_correction_type   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.560
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             846
_exptl_crystal_size_max          .31
_exptl_crystal_size_mid          .14
_exptl_crystal_size_min          .10
_refine_diff_density_max         1.128
_refine_diff_density_min         -1.082
_refine_diff_density_rms         0.129
_refine_ls_extinction_method     hand
_refine_ls_goodness_of_fit_ref   1.031
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     397
_refine_ls_number_reflns         5135
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.031
_refine_ls_R_factor_all          0.0463
_refine_ls_R_factor_gt           0.0382
_refine_ls_shift/su_max          0.410
_refine_ls_shift/su_mean         0.009
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0781P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1040
_refine_ls_wR_factor_ref         0.1076
_reflns_number_gt                4417
_reflns_number_total             5135
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b107072j.txt
_cod_data_source_block           15
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1824.11(4)
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C30.50 H35 Cl3 N2 O4 P2 Pt'
_cod_database_code               7011050
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.05832(3) 0.48656(2) 0.252119(17) 0.04097(13) Uani 1 1 d . . .
Cl1 Cl 0.03197(18) 0.67323(15) 0.22563(12) 0.0477(4) Uani 1 1 d . . .
Cl2 Cl -0.18236(17) 0.41072(15) 0.25975(11) 0.0460(4) Uani 1 1 d . . .
N1 N 0.2741(7) 0.3482(6) 0.2937(4) 0.0517(15) Uani 1 1 d . . .
C29 C 0.3661(9) 0.3417(10) 0.3696(6) 0.075(3) Uani 1 1 d . . .
H29A H 0.3167 0.2832 0.3996 0.112 Uiso 1 1 calc R . .
H29B H 0.4006 0.4179 0.4064 0.112 Uiso 1 1 calc R . .
H29C H 0.4425 0.3197 0.3534 0.112 Uiso 1 1 calc R . .
N2 N 0.3381(6) 0.4312(5) 0.2449(4) 0.0514(15) Uani 1 1 d . . .
C30 C 0.4143(11) 0.3865(9) 0.1872(7) 0.077(3) Uani 1 1 d . . .
H30A H 0.4553 0.4477 0.1564 0.116 Uiso 1 1 calc R . .
H30B H 0.3521 0.3189 0.1472 0.116 Uiso 1 1 calc R . .
H30C H 0.4859 0.3633 0.2199 0.116 Uiso 1 1 calc R . .
P1 P 0.1015(2) 0.32249(16) 0.28219(12) 0.0444(4) Uani 1 1 d . . .
C1 C 0.0178(9) 0.1920(7) 0.2007(5) 0.0534(19) Uani 1 1 d . . .
C2 C 0.0523(10) 0.0861(7) 0.2038(6) 0.066(2) Uani 1 1 d . . .
O2 O 0.1531(7) 0.0897(5) 0.2696(4) 0.0729(17) Uani 1 1 d . . .
C3 C -0.0179(13) -0.0142(8) 0.1398(7) 0.088(3) Uani 1 1 d . . .
H3A H 0.0055 -0.0839 0.1408 0.105 Uiso 1 1 calc R . .
C4 C -0.1194(14) -0.0089(10) 0.0767(8) 0.102(4) Uani 1 1 d . . .
H4A H -0.1672 -0.0763 0.0357 0.123 Uiso 1 1 calc R . .
C5 C -0.1532(12) 0.0928(10) 0.0719(7) 0.092(3) Uani 1 1 d . . .
H5A H -0.2214 0.0947 0.0268 0.110 Uiso 1 1 calc R . .
C6 C -0.0865(10) 0.1946(8) 0.1341(5) 0.067(2) Uani 1 1 d . . .
H6A H -0.1113 0.2633 0.1312 0.081 Uiso 1 1 calc R . .
C7 C 0.1810(15) -0.0231(10) 0.2779(10) 0.123(5) Uani 1 1 d . . .
H7A H 0.2547 -0.0106 0.3265 0.185 Uiso 1 1 calc R . .
H7B H 0.2076 -0.0515 0.2267 0.185 Uiso 1 1 calc R . .
H7C H 0.0989 -0.0808 0.2860 0.185 Uiso 1 1 calc R . .
C8 C 0.0510(8) 0.2780(7) 0.3797(5) 0.0493(18) Uani 1 1 d . . .
C9 C 0.0986(8) 0.3612(7) 0.4582(5) 0.0528(19) Uani 1 1 d . . .
O9 O 0.1901(7) 0.4681(5) 0.4552(3) 0.0682(16) Uani 1 1 d . . .
C10 C 0.0537(9) 0.3307(9) 0.5315(5) 0.064(2) Uani 1 1 d . . .
H10A H 0.0843 0.3860 0.5821 0.076 Uiso 1 1 calc R . .
C11 C -0.0361(10) 0.2190(9) 0.5310(6) 0.075(3) Uani 1 1 d . . .
H11A H -0.0626 0.1976 0.5814 0.090 Uiso 1 1 calc R . .
C12 C -0.0857(10) 0.1401(10) 0.4551(7) 0.083(3) Uani 1 1 d . . .
H12A H -0.1500 0.0661 0.4534 0.099 Uiso 1 1 calc R . .
C13 C -0.0407(9) 0.1700(8) 0.3816(6) 0.068(2) Uani 1 1 d . . .
H13A H -0.0741 0.1143 0.3312 0.081 Uiso 1 1 calc R . .
C14 C 0.2529(15) 0.5480(10) 0.5336(6) 0.107(4) Uani 1 1 d . . .
H14A H 0.3152 0.6195 0.5225 0.160 Uiso 1 1 calc R . .
H14B H 0.3035 0.5116 0.5717 0.160 Uiso 1 1 calc R . .
H14C H 0.1824 0.5671 0.5598 0.160 Uiso 1 1 calc R . .
P2 P 0.2775(2) 0.54739(16) 0.23872(12) 0.0437(4) Uani 1 1 d . . .
C15 C 0.3906(7) 0.6683(7) 0.3229(5) 0.0487(18) Uani 1 1 d . . .
C16 C 0.5348(9) 0.7021(8) 0.3314(6) 0.060(2) Uani 1 1 d . . .
O16 O 0.5792(6) 0.6447(6) 0.2696(5) 0.0790(19) Uani 1 1 d . . .
C17 C 0.6210(10) 0.7885(9) 0.3987(7) 0.073(3) Uani 1 1 d . . .
H17A H 0.7168 0.8072 0.4056 0.088 Uiso 1 1 calc R . .
C18 C 0.5655(11) 0.8459(9) 0.4547(7) 0.080(3) Uani 1 1 d . . .
H18A H 0.6239 0.9072 0.4976 0.096 Uiso 1 1 calc R . .
C19 C 0.4204(10) 0.8140(8) 0.4488(6) 0.073(3) Uani 1 1 d . . .
H19A H 0.3831 0.8512 0.4889 0.088 Uiso 1 1 calc R . .
C20 C 0.3342(9) 0.7254(7) 0.3817(5) 0.059(2) Uani 1 1 d . . .
H20A H 0.2385 0.7044 0.3763 0.071 Uiso 1 1 calc R . .
C21 C 0.7185(11) 0.6969(13) 0.2568(8) 0.103(4) Uani 1 1 d . . .
H21A H 0.7361 0.6469 0.2113 0.155 Uiso 1 1 calc R . .
H21B H 0.7836 0.7042 0.3088 0.155 Uiso 1 1 calc R . .
H21C H 0.7283 0.7742 0.2416 0.155 Uiso 1 1 calc R . .
C22 C 0.3030(8) 0.5966(6) 0.1377(5) 0.0487(17) Uani 1 1 d . . .
C23 C 0.2360(9) 0.5193(7) 0.0599(5) 0.059(2) Uani 1 1 d . . .
O23 O 0.1586(7) 0.4068(5) 0.0671(4) 0.0788(19) Uani 1 1 d . . .
C24 C 0.2521(11) 0.5558(9) -0.0182(6) 0.078(3) Uani 1 1 d . . .
H24A H 0.2073 0.5047 -0.0697 0.093 Uiso 1 1 calc R . .
C25 C 0.3362(12) 0.6698(9) -0.0177(6) 0.082(3) Uani 1 1 d . . .
H25A H 0.3508 0.6936 -0.0698 0.098 Uiso 1 1 calc R . .
C26 C 0.3982(12) 0.7480(9) 0.0561(6) 0.081(3) Uani 1 1 d . . .
H26A H 0.4522 0.8251 0.0548 0.098 Uiso 1 1 calc R . .
C27 C 0.3797(9) 0.7109(7) 0.1337(6) 0.060(2) Uani 1 1 d . . .
H27A H 0.4202 0.7648 0.1845 0.072 Uiso 1 1 calc R . .
C28 C 0.096(2) 0.3242(11) -0.0112(8) 0.159(8) Uani 1 1 d . . .
H28A H 0.0444 0.2493 0.0016 0.239 Uiso 1 1 calc R . .
H28B H 0.1672 0.3133 -0.0406 0.239 Uiso 1 1 calc R . .
H28C H 0.0350 0.3547 -0.0471 0.239 Uiso 1 1 calc R . .
C40 C 0.5868(15) 1.1150(13) 0.2186(8) 0.119(10) Uani 0.50 1 d PD . .
H40A H 0.6733 1.1193 0.2001 0.143 Uiso 0.50 1 calc PR . .
H40B H 0.5960 1.1939 0.2474 0.143 Uiso 0.50 1 calc PR . .
Cl3 Cl 0.4590(6) 1.0802(4) 0.1293(3) 0.0808(14) Uani 0.50 1 d PD . .
Cl4 Cl 0.5674(6) 1.0218(5) 0.2920(4) 0.109(2) Uani 0.50 1 d PD . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Pt1 P1 85.05(7) . . ?
P2 Pt1 Cl1 90.81(6) . . ?
P1 Pt1 Cl1 175.03(7) . . ?
P2 Pt1 Cl2 176.56(6) . . ?
P1 Pt1 Cl2 93.29(7) . . ?
Cl1 Pt1 Cl2 90.98(6) . . ?
N2 N1 C29 113.6(6) . . ?
N2 N1 P1 114.0(4) . . ?
C29 N1 P1 126.0(6) . . ?
N1 N2 C30 114.1(6) . . ?
N1 N2 P2 115.5(5) . . ?
C30 N2 P2 127.5(6) . . ?
N1 P1 C8 108.0(3) . . ?
N1 P1 C1 107.2(4) . . ?
C8 P1 C1 104.6(4) . . ?
N1 P1 Pt1 107.5(2) . . ?
C8 P1 Pt1 114.1(3) . . ?
C1 P1 Pt1 115.1(3) . . ?
C6 C1 C2 119.0(8) . . ?
C6 C1 P1 119.4(6) . . ?
C2 C1 P1 121.7(6) . . ?
O2 C2 C3 124.5(9) . . ?
O2 C2 C1 115.9(7) . . ?
C3 C2 C1 119.6(9) . . ?
C2 O2 C7 116.2(7) . . ?
C4 C3 C2 119.8(10) . . ?
C3 C4 C5 121.5(9) . . ?
C4 C5 C6 120.7(10) . . ?
C5 C6 C1 119.4(9) . . ?
C13 C8 C9 116.9(7) . . ?
C13 C8 P1 123.1(6) . . ?
C9 C8 P1 119.8(6) . . ?
O9 C9 C10 123.6(8) . . ?
O9 C9 C8 116.1(7) . . ?
C10 C9 C8 120.2(8) . . ?
C9 O9 C14 118.0(7) . . ?
C11 C10 C9 120.8(8) . . ?
C12 C11 C10 119.2(9) . . ?
C11 C12 C13 120.2(9) . . ?
C8 C13 C12 122.6(9) . . ?
N2 P2 C22 107.5(3) . . ?
N2 P2 C15 106.7(3) . . ?
C22 P2 C15 106.0(3) . . ?
N2 P2 Pt1 107.2(2) . . ?
C22 P2 Pt1 114.4(3) . . ?
C15 P2 Pt1 114.5(3) . . ?
C20 C15 C16 119.0(7) . . ?
C20 C15 P2 120.1(6) . . ?
C16 C15 P2 120.8(6) . . ?
O16 C16 C15 114.6(7) . . ?
O16 C16 C17 124.6(8) . . ?
C15 C16 C17 120.8(9) . . ?
C16 O16 C21 118.4(8) . . ?
C18 C17 C16 119.9(9) . . ?
C17 C18 C19 121.0(9) . . ?
C18 C19 C20 118.6(9) . . ?
C15 C20 C19 120.5(8) . . ?
C27 C22 C23 117.9(7) . . ?
C27 C22 P2 122.3(6) . . ?
C23 C22 P2 119.7(6) . . ?
O23 C23 C24 123.4(8) . . ?
O23 C23 C22 115.8(7) . . ?
C24 C23 C22 120.7(8) . . ?
C23 O23 C28 116.8(8) . . ?
C25 C24 C23 118.5(9) . . ?
C24 C25 C26 122.2(9) . . ?
C27 C26 C25 118.7(9) . . ?
C26 C27 C22 121.9(8) . . ?
Cl4 C40 Cl3 117.3(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 P2 2.2119(19) . ?
Pt1 P1 2.2137(19) . ?
Pt1 Cl1 2.3933(16) . ?
Pt1 Cl2 2.4047(17) . ?
N1 N2 1.407(9) . ?
N1 C29 1.440(10) . ?
N1 P1 1.688(7) . ?
N2 C30 1.452(10) . ?
N2 P2 1.682(6) . ?
P1 C8 1.807(7) . ?
P1 C1 1.806(7) . ?
C1 C6 1.395(12) . ?
C1 C2 1.411(12) . ?
C2 O2 1.342(11) . ?
C2 C3 1.409(13) . ?
O2 C7 1.469(12) . ?
C3 C4 1.352(16) . ?
C4 C5 1.362(16) . ?
C5 C6 1.398(13) . ?
C8 C13 1.364(11) . ?
C8 C9 1.427(11) . ?
C9 O9 1.358(10) . ?
C9 C10 1.375(11) . ?
O9 C14 1.417(10) . ?
C10 C11 1.380(13) . ?
C11 C12 1.371(14) . ?
C12 C13 1.376(13) . ?
P2 C22 1.812(8) . ?
P2 C15 1.824(8) . ?
C15 C20 1.393(11) . ?
C15 C16 1.399(11) . ?
C16 O16 1.350(11) . ?
C16 C17 1.386(13) . ?
O16 C21 1.444(11) . ?
C17 C18 1.357(14) . ?
C18 C19 1.414(14) . ?
C19 C20 1.395(12) . ?
C22 C27 1.375(11) . ?
C22 C23 1.403(11) . ?
C23 O23 1.374(10) . ?
C23 C24 1.387(12) . ?
O23 C28 1.429(12) . ?
C24 C25 1.380(13) . ?
C25 C26 1.354(13) . ?
C26 C27 1.385(12) . ?
C40 Cl4 1.7001(10) . ?
C40 Cl3 1.6999(10) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C29 N1 N2 C30 82.6(9) . . . . ?
P1 N1 N2 C30 -123.8(7) . . . . ?
C29 N1 N2 P2 -115.2(7) . . . . ?
P1 N1 N2 P2 38.4(7) . . . . ?
N2 N1 P1 C8 -152.6(5) . . . . ?
C29 N1 P1 C8 -2.9(8) . . . . ?
N2 N1 P1 C1 95.2(5) . . . . ?
C29 N1 P1 C1 -115.1(8) . . . . ?
N2 N1 P1 Pt1 -29.0(5) . . . . ?
C29 N1 P1 Pt1 120.7(7) . . . . ?
P2 Pt1 P1 N1 9.3(2) . . . . ?
Cl1 Pt1 P1 N1 -24.3(8) . . . . ?
Cl2 Pt1 P1 N1 -173.7(2) . . . . ?
P2 Pt1 P1 C8 129.0(3) . . . . ?
Cl1 Pt1 P1 C8 95.5(8) . . . . ?
Cl2 Pt1 P1 C8 -54.0(3) . . . . ?
P2 Pt1 P1 C1 -110.0(3) . . . . ?
Cl1 Pt1 P1 C1 -143.6(8) . . . . ?
Cl2 Pt1 P1 C1 67.0(3) . . . . ?
N1 P1 C1 C6 -131.7(7) . . . . ?
C8 P1 C1 C6 113.8(7) . . . . ?
Pt1 P1 C1 C6 -12.2(8) . . . . ?
N1 P1 C1 C2 50.1(8) . . . . ?
C8 P1 C1 C2 -64.4(8) . . . . ?
Pt1 P1 C1 C2 169.6(6) . . . . ?
C6 C1 C2 O2 -179.8(8) . . . . ?
P1 C1 C2 O2 -1.6(11) . . . . ?
C6 C1 C2 C3 0.4(14) . . . . ?
P1 C1 C2 C3 178.6(8) . . . . ?
C3 C2 O2 C7 -5.7(15) . . . . ?
C1 C2 O2 C7 174.6(9) . . . . ?
O2 C2 C3 C4 179.1(11) . . . . ?
C1 C2 C3 C4 -1.2(17) . . . . ?
C2 C3 C4 C5 2(2) . . . . ?
C3 C4 C5 C6 -2(2) . . . . ?
C4 C5 C6 C1 1.3(17) . . . . ?
C2 C1 C6 C5 -0.5(14) . . . . ?
P1 C1 C6 C5 -178.8(8) . . . . ?
N1 P1 C8 C13 -118.8(7) . . . . ?
C1 P1 C8 C13 -4.9(8) . . . . ?
Pt1 P1 C8 C13 121.7(7) . . . . ?
N1 P1 C8 C9 66.6(7) . . . . ?
C1 P1 C8 C9 -179.4(6) . . . . ?
Pt1 P1 C8 C9 -52.8(7) . . . . ?
C13 C8 C9 O9 179.8(7) . . . . ?
P1 C8 C9 O9 -5.3(10) . . . . ?
C13 C8 C9 C10 1.0(12) . . . . ?
P1 C8 C9 C10 175.8(6) . . . . ?
C10 C9 O9 C14 6.3(13) . . . . ?
C8 C9 O9 C14 -172.5(9) . . . . ?
O9 C9 C10 C11 -177.9(9) . . . . ?
C8 C9 C10 C11 0.9(13) . . . . ?
C9 C10 C11 C12 -3.1(15) . . . . ?
C10 C11 C12 C13 3.4(16) . . . . ?
C9 C8 C13 C12 -0.7(14) . . . . ?
P1 C8 C13 C12 -175.4(8) . . . . ?
C11 C12 C13 C8 -1.5(16) . . . . ?
N1 N2 P2 C22 -151.6(5) . . . . ?
C30 N2 P2 C22 7.7(9) . . . . ?
N1 N2 P2 C15 95.0(6) . . . . ?
C30 N2 P2 C15 -105.6(8) . . . . ?
N1 N2 P2 Pt1 -28.2(6) . . . . ?
C30 N2 P2 Pt1 131.2(7) . . . . ?
P1 Pt1 P2 N2 7.6(3) . . . . ?
Cl1 Pt1 P2 N2 -175.1(3) . . . . ?
Cl2 Pt1 P2 N2 -53.6(11) . . . . ?
P1 Pt1 P2 C22 126.7(3) . . . . ?
Cl1 Pt1 P2 C22 -56.0(3) . . . . ?
Cl2 Pt1 P2 C22 65.5(11) . . . . ?
P1 Pt1 P2 C15 -110.6(3) . . . . ?
Cl1 Pt1 P2 C15 66.7(3) . . . . ?
Cl2 Pt1 P2 C15 -171.8(11) . . . . ?
N2 P2 C15 C20 -127.1(7) . . . . ?
C22 P2 C15 C20 118.5(7) . . . . ?
Pt1 P2 C15 C20 -8.6(7) . . . . ?
N2 P2 C15 C16 50.4(7) . . . . ?
C22 P2 C15 C16 -63.9(7) . . . . ?
Pt1 P2 C15 C16 168.9(5) . . . . ?
C20 C15 C16 O16 -177.7(8) . . . . ?
P2 C15 C16 O16 4.7(10) . . . . ?
C20 C15 C16 C17 1.9(12) . . . . ?
P2 C15 C16 C17 -175.7(7) . . . . ?
C15 C16 O16 C21 161.1(8) . . . . ?
C17 C16 O16 C21 -18.5(13) . . . . ?
O16 C16 C17 C18 176.1(9) . . . . ?
C15 C16 C17 C18 -3.5(13) . . . . ?
C16 C17 C18 C19 4.0(15) . . . . ?
C17 C18 C19 C20 -2.8(14) . . . . ?
C16 C15 C20 C19 -0.8(12) . . . . ?
P2 C15 C20 C19 176.8(7) . . . . ?
C18 C19 C20 C15 1.2(14) . . . . ?
N2 P2 C22 C27 -122.0(7) . . . . ?
C15 P2 C22 C27 -8.2(8) . . . . ?
Pt1 P2 C22 C27 119.0(6) . . . . ?
N2 P2 C22 C23 62.2(7) . . . . ?
C15 P2 C22 C23 176.1(6) . . . . ?
Pt1 P2 C22 C23 -56.7(7) . . . . ?
C27 C22 C23 O23 -178.9(7) . . . . ?
P2 C22 C23 O23 -2.9(11) . . . . ?
C27 C22 C23 C24 2.9(13) . . . . ?
P2 C22 C23 C24 178.9(7) . . . . ?
C24 C23 O23 C28 1.9(16) . . . . ?
C22 C23 O23 C28 -176.3(11) . . . . ?
O23 C23 C24 C25 -177.8(9) . . . . ?
C22 C23 C24 C25 0.3(15) . . . . ?
C23 C24 C25 C26 -2.9(17) . . . . ?
C24 C25 C26 C27 2.0(18) . . . . ?
C25 C26 C27 C22 1.5(16) . . . . ?
C23 C22 C27 C26 -3.9(13) . . . . ?
P2 C22 C27 C26 -179.7(8) . . . . ?
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1 PubChem 139154434
