Information card for entry 7011560

Structure parameters

• Formula: C24 H28 Cl2 N4 O10 Pb
• Calculated formula: C24 H28 Cl2 N4 O10 Pb
• SMILES: [Pb]123Oc4c5C=[NH+]CCC[NH+]=Cc6cc(cc(C=[N]3CCC[N]2=Cc4cc(c5)C)c6O1)C.Cl(=O)(=O)(=O)[O-].Cl(=O)(=O)(=O)[O-]
• Title of publication: Organized assemblies of lead(ii) complexes of a tetraiminodiphenol macrocyclic ligand: manifestation of weak metal‒anion interactions and the directional influence of anions
• Authors of publication: Dutta, Bula; Adhikary, Bibhutosh; Bag, Pradip; Flörke, Ulrich; Nag, Kamalaksha
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 13
• Pages of publication: 2760
• a: 35.124 ± 0.005 Å
• b: 35.124 ± 0.005 Å
• c: 12.095 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 12922 ± 5 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.2748
• Residual factor for significantly intense reflections: 0.0748
• Weighted residual factors for significantly intense reflections: 0.1429
• Weighted residual factors for all reflections included in the refinement: 0.2227
• Goodness-of-fit parameter for all reflections included in the refinement: 0.866
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No