Information card for entry 7011602

Structure parameters

• Common name: complex 2
• Formula: C11.5 H23 Cl N3 S3 V
• Calculated formula: C11.51 H22 Cl N3 S3 V
• Title of publication: Synthesis, structure and chemistry of vanadium(iv) and vanadium(v) compounds with substituted hydrazido(1‒) and hydrazido(2‒) ligands
• Authors of publication: Davies, Sian C.; Hughes, David L.; Konkol, Martin; Richards, Raymond L.; Sanders, J. Roger; Sobota, Piotr
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 14
• Pages of publication: 2811
• a: 11.466 ± 0.001 Å
• b: 11.9468 ± 0.0012 Å
• c: 12.8618 ± 0.0013 Å
• α: 90°
• β: 91.595 ± 0.008°
• γ: 90°
• Cell volume: 1761.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.0565
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for all reflections: 0.1165
• Weighted residual factors for significantly intense reflections: 0.1025
• Goodness-of-fit parameter for all reflections: 1.056
• Goodness-of-fit parameter for significantly intense reflections: 1.102
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No