Crystallography Open Database

Information card for entry 7011630

Preview

Coordinates	7011630.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20.5 H19 Cl N2 O12 Ru4
Calculated formula	C20.5 H19 Cl N2 O12 Ru4
Title of publication	Synthesis of carbido and related derivatives from calcium carbide and ruthenium carbonyl clusters
Authors of publication	Bruce, Michael I.; Zaitseva, Natasha N.; Skelton, Brian W.; White, Allan H.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	20
Pages of publication	3879
a	13.2174 ± 0.0006 Å
b	14.5234 ± 0.0009 Å
c	16.571 ± 0.0007 Å
α	73.859 ± 0.001°
β	82.855 ± 0.001°
γ	68.495 ± 0.001°
Cell volume	2842 ± 0.3 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.06
Residual factor for significantly intense reflections	0.031
Weighted residual factors for all reflections	0.029
Weighted residual factors for all reflections included in the refinement	0.026
Goodness-of-fit parameter for all reflections	0.959
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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