Information card for entry 7011714

Structure parameters

• Formula: C20 H18 N4 O15 P2 V4
• Calculated formula: C20 H18 N4 O15 P2 V4
• Title of publication: Hydrothermal synthesis and crystal structure of a layered vanadium phosphate with a directly coordinated organonitrogen ligand: [V4O7(HPO4)2(2,2'-bipy)2]
• Authors of publication: Lu, Ying; Wang, Enbo; Yuan, Mei; Luan, Guoyou; Li, Yangguang; Zhang, Hong; Hu, Changwen; Yao, Yuangen; Qin, Yeyan; Chen, Yubiao
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 15
• Pages of publication: 3029
• a: 8.3682 ± 0.0017 Å
• b: 9.2153 ± 0.0018 Å
• c: 9.5991 ± 0.0019 Å
• α: 97.04 ± 0.03°
• β: 109.91 ± 0.03°
• γ: 99.01 ± 0.03°
• Cell volume: 675 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0534
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.1164
• Weighted residual factors for all reflections included in the refinement: 0.1225
• Goodness-of-fit parameter for all reflections included in the refinement: 0.937
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No