Information card for entry 7012165

Structure parameters

• Formula: C21 H29 Cl N2 O15 Os5
• Calculated formula: C21 H29 Cl N2 O15 Os5
• Title of publication: Tetraosmium carbonyl clusters containing µ-NH2 amido ligands: syntheses, crystal structures and reactivities
• Authors of publication: Li, Yat; Wong, Wing-Tak
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 3
• Pages of publication: 398
• a: 10.022 ± 0.001 Å
• b: 14.121 ± 0.001 Å
• c: 15.772 ± 0.002 Å
• α: 104.16 ± 0.01°
• β: 96.08 ± 0.02°
• γ: 107.32 ± 0.01°
• Cell volume: 2027.2 ± 0.4 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for all reflections included in the refinement: 0.0908
• Goodness-of-fit parameter for all reflections included in the refinement: 1.964
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No