Information card for entry 7012396

Structure parameters

• Formula: C18 H26 Cl N8 O2 Re S2
• Calculated formula: C18 H26 Cl0.5 N8 O2 Re0.5 S2
• Title of publication: Synthesis and characterisation of new homoleptic rhenium thiosemicarbazone complexes
• Authors of publication: Cowley, Andrew R.; Dilworth, Jonathan R.; Donnelly, Paul S.; Woollard-Shore, John
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 4
• Pages of publication: 748
• a: 8.6587 ± 0.0002 Å
• b: 12.7664 ± 0.0002 Å
• c: 21.9866 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2430.41 ± 0.08 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for significantly intense reflections: 0.0197
• Weighted residual factors for all reflections included in the refinement: 0.0259
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No