Information card for entry 7012447

Structure parameters

• Formula: C53 H50.5 Co2 F18 N8 O8.25 P3
• Calculated formula: C53 H44 Co2 F18 N8 O8.25 P3
• Title of publication: The effect of phenyl substituents on supramolecular assemblies containing directly linked bis-pyridylimine ligands: synthesis and structural characterisation of mononuclear nickel(ii) and dinuclear silver(i) and cobalt(iii) complexes of (2-pyridyl)phenylketazine
• Authors of publication: Tuna, Floriana; Clarkson, Guy; Alcock, Nathaniel W.; Hannon, Michael J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2149
• a: 12.2068 ± 0.0018 Å
• b: 13.2943 ± 0.0019 Å
• c: 21.456 ± 0.003 Å
• α: 80.385 ± 0.003°
• β: 82.541 ± 0.003°
• γ: 73.978 ± 0.003°
• Cell volume: 3286.7 ± 0.8 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1671
• Residual factor for significantly intense reflections: 0.0763
• Weighted residual factors for significantly intense reflections: 0.166
• Weighted residual factors for all reflections included in the refinement: 0.2066
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No