Information card for entry 7012475

Structure parameters

• Formula: C32 H22 Fe O12 Os3 P
• Calculated formula: C32 H22 Fe O12 Os3 P
• Title of publication: Reaction of metallophosphanide anions with MLnX (X = halide) species as a simple route to heterometallic transition metal complexes
• Authors of publication: Birte Ahrens; Jacqueline M. Cole; Jonathan P. Hickey; James N. Martin; Martin J. Mays; Paul R. Raithby; Simon J. Teat; Anthony D. Woods
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 7
• Pages of publication: 1389 - 1395
• a: 8.9577 ± 0.0019 Å
• b: 10.834 ± 0.002 Å
• c: 34.169 ± 0.007 Å
• α: 90°
• β: 94.537 ± 0.01°
• γ: 90°
• Cell volume: 3305.6 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0786
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.0935
• Weighted residual factors for all reflections included in the refinement: 0.0973
• Goodness-of-fit parameter for all reflections included in the refinement: 1.178
• Diffraction radiation wavelength: 0.6923 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No