Information card for entry 7012857

Structure parameters

• Formula: C20 H106 Cu5 N20 O54 W12
• Calculated formula: C20 H106 Cu5 N20 O54 W12
• Title of publication: A new polymeric chain formed by paradodecatungstate clusters and [Cu(en)2]2+ complexes: hydrothermal synthesis and characterization of [Cu(en)2]3[{Cu(en)2}2(H2W12O42)]�12H2OElectronic supplementary information (ESI) available: thermal variations of the magnetic susceptibility of compound 1. See http://www.rsc.org/suppdata/dt/b3/b301917a/
• Authors of publication: Lin, Bi-Zhou; Chen, Yan-Min; Liu, Pei-De
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 12
• Pages of publication: 2474
• a: 12.1989 ± 0.0007 Å
• b: 14.0042 ± 0.0008 Å
• c: 14.7254 ± 0.0009 Å
• α: 62.144 ± 0.001°
• β: 67.294 ± 0.003°
• γ: 77.875 ± 0.002°
• Cell volume: 2050.4 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0345
• Residual factor for significantly intense reflections: 0.0275
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0767
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No