Information card for entry 7012860

Structure parameters

• Formula: Ce H76 Mo22 N11 O94 P2
• Calculated formula: Ce Mo22 N11 O94 P2
• Title of publication: A rare structural characterisation of the phosphomolybdate lacunary anion, [PMo~11~O~39~]^7-^. Crystal structures of the Ln(III) complexes, (NH~4~)~11~[Ln(PMo~11~O~39~)~2~]·16H~2~O (Ln = Ce^III^, Sm^III^, Dy^III^ or Lu^III^)
• Authors of publication: Gaunt, Andrew J.; May, Iain; Sarsfield, Mark J.; Collison, David; Helliwell, Madeleine; Denniss, Iain S.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 13
• Pages of publication: 2767 - 2771
• a: 38.035 ± 0.01 Å
• b: 13.106 ± 0.01 Å
• c: 19.84 ± 0.01 Å
• α: 90°
• β: 117.7 ± 0.03°
• γ: 90°
• Cell volume: 8757 ± 9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0844
• Weighted residual factors for all reflections included in the refinement: 0.0866
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No