Information card for entry 7012883

Structure parameters

• Common name: ((lithium)bis(penta(3,5- dimethylphenyl)cyclopentadienide)(lithium) bis(tetramethylethylenediamine))
• Chemical name: [(lithium)bis(penta(3,5-dimethylphenyl)cyclopentadienide][lithium) bis(tetramethylethylenediamine)]
• Formula: C110 H138 Li3 N4 O4
• Calculated formula: C102 H122 Li2 N4
• Title of publication: Synthesis, structure and solution dynamics of lithium salts of superbulky cyclopentadienyl ligands
• Authors of publication: Giesbrecht, Garth R.; Gordon, John C.; Clark, David L.; Scott, Brian L.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 13
• Pages of publication: 2658
• a: 14.216 ± 0.004 Å
• b: 20.023 ± 0.005 Å
• c: 22.771 ± 0.006 Å
• α: 98.14 ± 0.006°
• β: 106.914 ± 0.004°
• γ: 109.938 ± 0.005°
• Cell volume: 5617 ± 3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.14
• Residual factor for significantly intense reflections: 0.0962
• Weighted residual factors for significantly intense reflections: 0.2744
• Weighted residual factors for all reflections included in the refinement: 0.2954
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No