Information card for entry 7012953

Structure parameters

• Chemical name: PG Taylor
• Formula: C16 H36 O6 Si4
• Calculated formula: C16 H36 O6 Si4
• Title of publication: A higher yielding route for T8 silsesquioxane cages and X-ray crystal structures of some novel spherosilicates
• Authors of publication: Bassindale, Alan R.; Liu, Zhihua; MacKinnon, Iain A.; Taylor, Peter G.; Yang, Yuxing; Light, Mark E.; Horton, Peter N.; Hursthouse, Michael B.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 14
• Pages of publication: 2945
• a: 9.9881 ± 0.0013 Å
• b: 10.8183 ± 0.0014 Å
• c: 10.954 ± 0.0018 Å
• α: 96.541 ± 0.008°
• β: 91.269 ± 0.007°
• γ: 99.439 ± 0.007°
• Cell volume: 1159 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2189
• Residual factor for significantly intense reflections: 0.0841
• Weighted residual factors for significantly intense reflections: 0.1572
• Weighted residual factors for all reflections included in the refinement: 0.2024
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No