Information card for entry 7013080

Structure parameters

• Common name: Bedford
• Formula: C32 H24.25 F12 N O2.25 P Pd
• Calculated formula: C32 H24.25 F12 N O2.25 P Pd
• Title of publication: Phosphine and arsine adducts of N-donor palladacycles as catalysts in the Suzuki coupling of aryl bromides
• Authors of publication: Robin B. Bedford; Catherine S. J. Cazin; Simon J. Coles; Thomas Gelbrich; Michael B. Hursthouse; Véronique J. M. Scordia
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 17
• Pages of publication: 3350 - 3356
• a: 10.0804 ± 0.0001 Å
• b: 11.7444 ± 0.0001 Å
• c: 14.4457 ± 0.0002 Å
• α: 74.069 ± 0.001°
• β: 83.998 ± 0.001°
• γ: 83.562 ± 0.001°
• Cell volume: 1629.27 ± 0.03 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.04
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0955
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No