Information card for entry 7013120

Structure parameters

• Formula: C20 H27 Cl2 N11 O8 Pb2
• Calculated formula: C20 H27 Cl2 N11 O8 Pb2
• Title of publication: Monomeric, trimeric and polymeric assemblies of dicopper(ii) complexes of a triazolate-containing Schiff-base macrocycleElectronic supplementary information (ESI) available: Geometric data for complexes 1?6. See http://www.rsc.org/suppdata/dt/b3/b304658c/
• Authors of publication: Depree, Craig V.; Beckmann, Udo; Heslop, Katie; Brooker, Sally
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 15
• Pages of publication: 3071
• a: 12.025 ± 0.005 Å
• b: 11.018 ± 0.005 Å
• c: 21.943 ± 0.005 Å
• α: 90 ± 0.005°
• β: 94.246 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 2899.3 ± 1.9 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0491
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0993
• Weighted residual factors for all reflections included in the refinement: 0.1044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No