Information card for entry 7013264

Structure parameters

• Formula: C20 H49 Lu O4 Si3
• Calculated formula: C20 H49 Lu O4 Si3
• SMILES: [Lu]123([O]4CC[O]1CC[O]2CC[O]3CC4)(C[Si](C)(C)C)(C[Si](C)(C)C)C[Si](C)(C)C
• Title of publication: Neutral and cationic trimethylsilylmethyl complexes of the rare earth metals supported by a crown ether: synthesis and structural characterization
• Authors of publication: Arndt, Stefan; Zeimentz, Peter M.; Spaniol, Thomas P.; Okuda, Jun; Honda, Masaru; Tatsumi, Kazuyuki
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3622
• a: 9.753 ± 0.004 Å
• b: 16.163 ± 0.002 Å
• c: 19.119 ± 0.003 Å
• α: 90°
• β: 99.24 ± 0.02°
• γ: 90°
• Cell volume: 2974.8 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1903
• Residual factor for significantly intense reflections: 0.0818
• Weighted residual factors for significantly intense reflections: 0.174
• Weighted residual factors for all reflections included in the refinement: 0.2129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No