Crystallography Open Database

Information card for entry 7013276

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Structure parameters

Formula	C27 H32 N P
Calculated formula	C27 H32 N P
SMILES	P(c1ccccc1)(c1ccccc1)C/C(=N/c1c(cccc1C(C)C)C(C)C)C
Title of publication	Nickel and palladium phosphinimine-imine ligand complexes
Authors of publication	Masuda, Jason D.; Wei, Pingrong; Stephan, Douglas W.
Journal of publication	Dalton Transactions
Year of publication	2003
Journal issue	18
Pages of publication	3500
a	21.355 ± 0.012 Å
b	17.586 ± 0.01 Å
c	13.052 ± 0.007 Å
α	90°
β	98.315 ± 0.012°
γ	90°
Cell volume	4850 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0766
Residual factor for significantly intense reflections	0.039
Weighted residual factors for significantly intense reflections	0.0925
Weighted residual factors for all reflections included in the refinement	0.1028
Goodness-of-fit parameter for all reflections included in the refinement	0.905
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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