Information card for entry 7013278

Structure parameters

• Formula: C47 H64 Br2 Li N2 Ni O2 P
• Calculated formula: C47 H56 Br2 Li N2 Ni O2 P
• Title of publication: Nickel and palladium phosphinimine-imine ligand complexes
• Authors of publication: Masuda, Jason D.; Wei, Pingrong; Stephan, Douglas W.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3500
• a: 11.284 ± 0.006 Å
• b: 13.404 ± 0.007 Å
• c: 18.234 ± 0.01 Å
• α: 81.631 ± 0.01°
• β: 74.457 ± 0.012°
• γ: 67.997 ± 0.009°
• Cell volume: 2460 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.178
• Residual factor for significantly intense reflections: 0.0671
• Weighted residual factors for significantly intense reflections: 0.1485
• Weighted residual factors for all reflections included in the refinement: 0.1909
• Goodness-of-fit parameter for all reflections included in the refinement: 0.906
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No