Information card for entry 7013292

Structure parameters

• Formula: C25.5 H21 Cl2 O P2 Rh
• Calculated formula: C25.5 H20 Cl2 O2 P2 Rh
• Title of publication: Synthesis and reactivity of rhodium(i) complexes containing keto-functionalised N-pyrrolyl phosphine ligands
• Authors of publication: Burrows, Andrew D.; Harrington, Ross W.; Mahon, Mary F.; Palmer, Mark T.; Senia, Francesco; Varrone, Maurizio
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 19
• Pages of publication: 3717
• a: 14.394 ± 0.002 Å
• b: 9.683 ± 0.002 Å
• c: 17.287 ± 0.003 Å
• α: 90°
• β: 92.93 ± 0.02°
• γ: 90°
• Cell volume: 2406.3 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.068
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.1165
• Weighted residual factors for all reflections included in the refinement: 0.1264
• Goodness-of-fit parameter for all reflections included in the refinement: 0.87
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No