Information card for entry 7013331

Structure parameters

• Formula: C16 H34 Cu2 N14 O4 W
• Calculated formula: C16 H16 Cu2 N14 O4 W
• Title of publication: Coordination polymers based on octacyanometalates(IV,V)(M = Mo, W) and aliphatic polyamine copper(II) tectons with [N3] donor atom sets
• Authors of publication: Robert Podgajny; Tomasz Korzeniak; Katarzyna Stadnicka; Yves Dromzée; Nathaniel W. Alcock; William Errington; Krzysztof Kruczała; Maria Bałanda; Terence J. Kemp; Michel Verdaguer; Barbara Sieklucka
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 17
• Pages of publication: 3458 - 3468
• a: 12.8799 ± 0.0001 Å
• b: 9.969 ± 0.0002 Å
• c: 11.3691 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1459.79 ± 0.04 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0473
• Residual factor for significantly intense reflections: 0.0347
• Weighted residual factors for significantly intense reflections: 0.0735
• Weighted residual factors for all reflections included in the refinement: 0.0806
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No