Information card for entry 7013334

Structure parameters

• Formula: C26 H42 Cl8 Rh2 S2
• Calculated formula: C26 H42 Cl8 Rh2 S2
• SMILES: [Rh]1234(Cl)(Cl)([S]5C[S]([Rh]6789(Cl)(Cl)[c]%10([c]6([c]7([c]8([c]9%10C)C)C)C)C)CCC5)[c]5([c]4([c]3([c]2([c]15C)C)C)C)C.ClCCl.ClCCl
• Title of publication: Preparation and characterization of rhodium(iii), iridium(iii) and ruthenium(ii) bearing 1,3- or 1,4-dithianesElectronic supplementary information (ESI) available: Crystal data and ORTEP figures for 2b, 2ab and 3c and further experimental details. See http://www.rsc.org/suppdata/dt/b3/b306496d/
• Authors of publication: Yamamoto, Yasuhiro; Sakamoto, Shinobu; Ohki, Yuka; Usuzawa, Akihiro; Fujita, Masanori; Mochida, Tomoyuki
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3534
• a: 14.068 ± 0.003 Å
• b: 9.243 ± 0.002 Å
• c: 15.487 ± 0.002 Å
• α: 90°
• β: 115.25 ± 0.01°
• γ: 90°
• Cell volume: 1821.4 ± 0.6 ų
• Cell temperature: 301.2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for all reflections included in the refinement: 0.1112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.43
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No