Information card for entry 7013339

Structure parameters

• Formula: C19 H33 Cl3 F6 P Rh S4
• Calculated formula: C19 H33 Cl3 F6 P Rh S4
• Title of publication: Preparation and characterization of rhodium(iii), iridium(iii) and ruthenium(ii) bearing 1,3- or 1,4-dithianesElectronic supplementary information (ESI) available: Crystal data and ORTEP figures for 2b, 2ab and 3c and further experimental details. See http://www.rsc.org/suppdata/dt/b3/b306496d/
• Authors of publication: Yamamoto, Yasuhiro; Sakamoto, Shinobu; Ohki, Yuka; Usuzawa, Akihiro; Fujita, Masanori; Mochida, Tomoyuki
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3534
• a: 12.79 ± 0.02 Å
• b: 12.114 ± 0.008 Å
• c: 19.49 ± 0.01 Å
• α: 90°
• β: 89.59 ± 0.08°
• γ: 90°
• Cell volume: 3020 ± 5 ų
• Cell temperature: 301.2 K
• Ambient diffraction temperature: 301.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1412
• Residual factor for significantly intense reflections: 0.1359
• Weighted residual factors for significantly intense reflections: 0.2156
• Weighted residual factors for all reflections included in the refinement: 0.223
• Goodness-of-fit parameter for all reflections included in the refinement: 2.023
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No