Information card for entry 7013347

Structure parameters

• Formula: C36 H62 P3 Rh Si
• Calculated formula: C36 H62 P3 Rh Si
• Title of publication: C?F Activation and hydrodefluorination of fluorinated alkenes at rhodiumBased on the presentation given at Dalton Discussion No. 6, 9?11th September 2003, University of York, UK.
• Authors of publication: Noveski, Daniel; Braun, Thomas; Schulte, Miriam; Neumann, Beate; Stammler, Hans-Georg
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 21
• Pages of publication: 4075
• a: 28.465 ± 0.003 Å
• b: 17.35 ± 0.0014 Å
• c: 22.7 ± 0.003 Å
• α: 90°
• β: 96.928 ± 0.011°
• γ: 90°
• Cell volume: 11129 ± 2 ų
• Cell temperature: 104 ± 2 K
• Ambient diffraction temperature: 104 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1171
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.0813
• Weighted residual factors for all reflections included in the refinement: 0.1139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No