Information card for entry 7013655

Structure parameters

• Formula: C61 H71 Cl2 N O9 P2 Pd
• Calculated formula: C61 H71 Cl2 N O9 P2 Pd
• Title of publication: Coordination chemistry and X-ray studies with novel sterically constrained diphosphonite ligands
• Authors of publication: van der Vlugt, Jarl Ivar; Sablong, Rafael; Mills, Allison M.; Kooijman, Huub; Spek, Anthony L.; Meetsma, Auke; Vogt, Dieter
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4690
• a: 11.5297 ± 0.0003 Å
• b: 20.7719 ± 0.0003 Å
• c: 24.2993 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5819.5 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0564
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for significantly intense reflections: 0.0758
• Weighted residual factors for all reflections included in the refinement: 0.0837
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No