Information card for entry 7013658

Structure parameters

• Formula: C56 H64 Cl O6 P2 Rh
• Calculated formula: C56 H64 Cl O6 P2 Rh
• Title of publication: Coordination chemistry and X-ray studies with novel sterically constrained diphosphonite ligands
• Authors of publication: van der Vlugt, Jarl Ivar; Sablong, Rafael; Mills, Allison M.; Kooijman, Huub; Spek, Anthony L.; Meetsma, Auke; Vogt, Dieter
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4690
• a: 16.8142 ± 0.001 Å
• b: 16.2527 ± 0.001 Å
• c: 18.5497 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5069.2 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0573
• Weighted residual factors for all reflections included in the refinement: 0.0616
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No