Information card for entry 7013660

Structure parameters

• Common name: Tetraoxotetrapyridinesquaratodimolybdenum(V) methanol pyridine (1/2/0.5)
• Chemical name: Tetraoxotetrapyridinesquaratodimolybdenum(V) methanol pyridine (1/2/0.5)
• Formula: C28.5 H30.5 Mo2 N4.5 O10
• Calculated formula: C28.5 H30.5 Mo2 N4.5 O10
• Title of publication: Novel molybdenum(V) squarato complexes based on the dinuclear metal‒metal bonded unit: syntheses and structural characterization of dinuclear [Mo2O4(C4O4)(R-Py)4] and tetranuclear [Mo4O8(C4O4)4]4−
• Authors of publication: Barbara Modec; Jurij V. Brenčič; Eric M. Burkholder; Jon Zubieta
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4618 - 4625
• a: 10.3502 ± 0.0002 Å
• b: 10.9722 ± 0.0001 Å
• c: 14.9631 ± 0.0002 Å
• α: 70.3901 ± 0.0006°
• β: 79.9458 ± 0.0006°
• γ: 86.485 ± 0.0006°
• Cell volume: 1576.13 ± 0.04 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0315
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0677
• Weighted residual factors for all reflections included in the refinement: 0.0704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.126
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No