Information card for entry 7013665

Structure parameters

• Common name: dichlorodimethoxooctaoxotetrapyridinetetramolybdenum(V) acetonitrile (1/1)
• Chemical name: dichlorodimethoxooctaoxotetrapyridinetetramolybdenum(V) acetonitrile (1/1)
• Formula: C24 H29 Cl2 Mo4 N5 O10
• Calculated formula: C24 H29 Cl2 Mo4 N5 O10
• Title of publication: Novel molybdenum(V) squarato complexes based on the dinuclear metal‒metal bonded unit: syntheses and structural characterization of dinuclear [Mo2O4(C4O4)(R-Py)4] and tetranuclear [Mo4O8(C4O4)4]4−
• Authors of publication: Barbara Modec; Jurij V. Brenčič; Eric M. Burkholder; Jon Zubieta
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4618 - 4625
• a: 25.566 ± 0.0005 Å
• b: 12.802 ± 0.0003 Å
• c: 10.1968 ± 0.0002 Å
• α: 90°
• β: 103.347 ± 0.0009°
• γ: 90°
• Cell volume: 3247.23 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0402
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0742
• Weighted residual factors for all reflections included in the refinement: 0.0793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No