Information card for entry 7013670

Structure parameters

• Formula: C39 H68 N O3 S2 Si2 Y
• Calculated formula: C39 H68 N O3 S2 Si2 Y
• Title of publication: Rare earth metal complexes supported by 1,ω-dithiaalkanediyl-bridged bis(phenolato) ligands: synthesis, characterization and ring-opening polymerization catalysis of l-lactide
• Authors of publication: Ma, Haiyan; Spaniol, Thomas P.; Okuda, Jun
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4770 - 4780
• a: 14.021 ± 0.003 Å
• b: 15.195 ± 0.004 Å
• c: 22.294 ± 0.003 Å
• α: 90°
• β: 98.23 ± 0.01°
• γ: 90°
• Cell volume: 4700.8 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2478
• Residual factor for significantly intense reflections: 0.0714
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.147
• Goodness-of-fit parameter for all reflections included in the refinement: 0.942
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No