Information card for entry 7013769

Structure parameters

• Common name: Chloro(2-methoxy-N-methylquinolin-4- yl)bis(triphenylphosphine) palladium(ii)
• Chemical name: Chloro(2-methoxy-N-methylquinolin-4-yl)bis(triphenylphosphine) palladium(II)
• Formula: C49 H45 B Cl5 F4 N O P2 Pd
• Calculated formula: C49 H45 B Cl5 F4 N O P2 Pd
• Title of publication: Preparation and characterisation of palladium, platinum and manganese di(organo)carbene complexes from quinolinone and quinolinium precursors.
• Authors of publication: Meyer, Wolfgang H.; Deetlefs, Maggel; Pohlmann, Michael; Scholz, Roland; Esterhuysen, Matthias W.; Julius, Gerrit R.; Raubenheimer, Helgard G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 3
• Pages of publication: 413 - 420
• a: 10.973 ± 0.001 Å
• b: 20.054 ± 0.001 Å
• c: 22.59 ± 0.001 Å
• α: 90 ± 0.01°
• β: 90 ± 0.01°
• γ: 90 ± 0.01°
• Cell volume: 4971 ± 0.6 ų
• Cell temperature: 175 ± 2 K
• Ambient diffraction temperature: 175 ± 2 K
• Number of distinct elements: 9
• Space group number: 57
• Hermann-Mauguin space group symbol: P b c m
• Hall space group symbol: -P 2c 2b
• Residual factor for all reflections: 0.0423
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No