Information card for entry 7014029

Structure parameters

• Chemical name: Iodobis(1,2-bis(dimethylstibanylmethyl)benzene)nickel(II) perchlorate
• Formula: C24 H40 Cl I Ni O4 Sb4
• Calculated formula: C24 H40 Cl I Ni O4 Sb4
• SMILES: [Ni]12(I)([Sb](C)(C)Cc3ccccc3C[Sb]1(C)C)[Sb](C)(C)Cc1ccccc1C[Sb]2(C)C.Cl(=O)(=O)(=O)[O-]
• Title of publication: Synthesis and characterisation of transition metal halide complexes of the xylyl-distibine, 1,2-bis(dimethylstibanylmethyl)benzene.
• Authors of publication: Levason, William; Matthews, Melissa L.; Reid, Gillian; Webster, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 4
• Pages of publication: 554 - 561
• a: 9.4616 ± 0.0015 Å
• b: 13.608 ± 0.003 Å
• c: 27.146 ± 0.004 Å
• α: 95.814 ± 0.01°
• β: 95.74 ± 0.01°
• γ: 107.789 ± 0.008°
• Cell volume: 3279.1 ± 1 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1123
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1387
• Weighted residual factors for all reflections included in the refinement: 0.1595
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No