Information card for entry 7014511

Structure parameters

• Common name: (K(2,2,2-crypt))6(In(P7)2)2*7py
• Chemical name: [K(2,2,2-crypt)]6[In(P7)2]2*7py
• Formula: C143 H251 In2 K6 N19 O36 P28
• Calculated formula: C143 H251 In2 K6 N19 O36 P28
• Title of publication: A versatile salt-metathesis route to heteroatomic clusters derived from phosphorus and arsenic Zintl anions.
• Authors of publication: Knapp, Caroline M.; Large, Joseph S.; Rees, Nicholas H.; Goicoechea, Jose M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 3
• Pages of publication: 735 - 745
• a: 15.9776 ± 0.0001 Å
• b: 25.1208 ± 0.0001 Å
• c: 27.1871 ± 0.0002 Å
• α: 113.86 ± 0.001°
• β: 94.394 ± 0.001°
• γ: 94.259 ± 0.001°
• Cell volume: 9883.66 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1057
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.1064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No