Information card for entry 7014515

Structure parameters

• Common name: (K(2,2,2-crypt))3(PbP15)*en
• Chemical name: [K(2,2,2-crypt)]3[PbP15]*en
• Formula: C56 H116 K3 N8 O18 P15 Pb
• Calculated formula: C56 H116.02 K3 N8 O18 P15 Pb
• Title of publication: A versatile salt-metathesis route to heteroatomic clusters derived from phosphorus and arsenic Zintl anions.
• Authors of publication: Knapp, Caroline M.; Large, Joseph S.; Rees, Nicholas H.; Goicoechea, Jose M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 3
• Pages of publication: 735 - 745
• a: 23.8547 ± 0.0002 Å
• b: 24.2093 ± 0.0002 Å
• c: 30.8457 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 17813.6 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 73
• Hermann-Mauguin space group symbol: I b c a
• Hall space group symbol: -I 2b 2c
• Residual factor for all reflections: 0.0947
• Residual factor for significantly intense reflections: 0.0847
• Weighted residual factors for significantly intense reflections: 0.1748
• Weighted residual factors for all reflections included in the refinement: 0.1779
• Goodness-of-fit parameter for all reflections included in the refinement: 1.172
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No