Stereochemically inactive lone pairs in phosphorus(iii) compounds: the characterisation of some derivatives with the 2,5-(CF(3))(2)C(6)H(3) (Ar) substituent and their complexation behaviour towards Pt(ii) species.
Authors of publication
Capel, Victoria L.; Dillon, Keith B.; Goeta, Andrés E; Howard, Judith A. K.; Monks, Philippa K.; Probert, Michael R.; Shepherd, Helena J.; Zorina, Natalia V.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
8
Pages of publication
1808 - 1816
a
16.1273 ± 0.0003 Å
b
8.2646 ± 0.0002 Å
c
25.3157 ± 0.0005 Å
α
90°
β
90°
γ
90°
Cell volume
3374.22 ± 0.12 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.0433
Residual factor for significantly intense reflections
0.0406
Weighted residual factors for significantly intense reflections
0.1079
Weighted residual factors for all reflections included in the refinement
0.11
Goodness-of-fit parameter for all reflections included in the refinement
