Crystallography Open Database

Information card for entry 7014972

Preview

Coordinates	7014972.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C77.5 H75 Cl3 F12 N6 O5 Os2 P4
Calculated formula	C77.5 H74 Cl3 F12 N6 O5 Os2 P4
Title of publication	Binuclear (salen)osmium phosphinidine and phosphiniminato complexes.
Authors of publication	Chen, Gui; Man, Wai-Lun; Yiu, Shek-Man; Wong, Tsz-Wing; Szeto, Lap; Wong, Wing-Tak; Lau, Tai-Chu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	9
Pages of publication	1938 - 1944
a	14.2178 ± 0.0003 Å
b	14.952 ± 0.0003 Å
c	20.6258 ± 0.0005 Å
α	69.1705 ± 0.0019°
β	84.0361 ± 0.0017°
γ	68.108 ± 0.0018°
Cell volume	3800.55 ± 0.16 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0588
Residual factor for significantly intense reflections	0.0455
Weighted residual factors for significantly intense reflections	0.1162
Weighted residual factors for all reflections included in the refinement	0.1215
Goodness-of-fit parameter for all reflections included in the refinement	0.968
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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