Information card for entry 7015327

Structure parameters

• Formula: C35 H56 N4 Ni4 O32
• Calculated formula: C35 H37 N4 Ni4 O32
• Title of publication: Two new 1,2,4,5-cyclohexanetetracarboxylate-bridged frameworks with metal hydroxide subunits. Synthesis, structures, magnetism and adsorption.
• Authors of publication: Ou, Yong-Cong; Wang, Jing; Leng, Ji-Dong; Lin, Zhuo-Jia; Tong, Ming-Liang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 14
• Pages of publication: 3592 - 3600
• a: 22.1211 ± 0.0012 Å
• b: 17.5536 ± 0.001 Å
• c: 7.048 ± 0.0005 Å
• α: 90°
• β: 97.06 ± 0.002°
• γ: 90°
• Cell volume: 2716 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0602
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1584
• Weighted residual factors for all reflections included in the refinement: 0.1637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No