Information card for entry 7015481

Structure parameters

• Formula: C53 H83 N5 O19 Pt15
• Calculated formula: C53 H83 N5 O19 Pt15
• Title of publication: The inter-conversions of platinum carbonyl dianionic clusters, [Pt3(CO)6](n)2- (n = 2-5), in THF and acetonitrile. A combined in situ FTIR spectroscopic and BTEM study leading to the characterization of the new [H(4-x)Pt15(CO)19]x- (x = 2-4) clusters.
• Authors of publication: Gao, F.; Li, C.; Heaton, B. T.; Zacchini, S.; Zarra, S.; Longoni, G.; Garland, M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 18
• Pages of publication: 5002 - 5008
• a: 12.93 ± 0.004 Å
• b: 14.224 ± 0.004 Å
• c: 22.326 ± 0.006 Å
• α: 84.783 ± 0.004°
• β: 88.519 ± 0.004°
• γ: 64.047 ± 0.004°
• Cell volume: 3676.3 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0856
• Residual factor for significantly intense reflections: 0.0593
• Weighted residual factors for significantly intense reflections: 0.1459
• Weighted residual factors for all reflections included in the refinement: 0.1637
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No