Tridentate complexes of 2,6-bis(4-substituted-1,2,3-triazol-1-ylmethyl)pyridine and its organic azide precursors: an application of the copper(II) acetate-accelerated azide-alkyne cycloaddition.
Authors of publication
Brotherton, Wendy S.; Guha, Pampa M.; Phan, Hoa; Clark, Ronald J.; Shatruk, Michael; Zhu, Lei
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
14
Pages of publication
3655 - 3665
a
15.5617 ± 0.0012 Å
b
11.3047 ± 0.0009 Å
c
7.9984 ± 0.0006 Å
α
90°
β
90°
γ
90°
Cell volume
1407.08 ± 0.19 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
60
Hermann-Mauguin space group symbol
P b c n
Hall space group symbol
-P 2n 2ab
Residual factor for all reflections
0.0266
Residual factor for significantly intense reflections
0.0233
Weighted residual factors for significantly intense reflections
0.0631
Weighted residual factors for all reflections included in the refinement
0.0651
Goodness-of-fit parameter for all reflections included in the refinement
