Synthesis, characterization, crystal structure and preliminary reactivity behaviour of new heteropolytopic ligands based on the 1,3,5-triazine spacer and pyrazolyl, tris-pyrazolylmethyl and tris-pyrazolylethoxy bonding fragments.
Authors of publication
Di Nicola, C.; Garau, F.; Marchetti, F.; Monari, M.; Pandolfo, L.; Pettinari, C.; Venzo, A.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
18
Pages of publication
4941 - 4953
a
8.8379 ± 0.0005 Å
b
11.6404 ± 0.0007 Å
c
18.3088 ± 0.0011 Å
α
80.857 ± 0.001°
β
85.384 ± 0.001°
γ
67.977 ± 0.001°
Cell volume
1723.48 ± 0.18 Å3
Cell temperature
273 ± 2 K
Ambient diffraction temperature
273 ± 2 K
Number of distinct elements
3
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1311
Residual factor for significantly intense reflections
0.0792
Weighted residual factors for significantly intense reflections
0.251
Weighted residual factors for all reflections included in the refinement
0.291
Goodness-of-fit parameter for all reflections included in the refinement
