Information card for entry 7015932

Structure parameters

• Formula: C9 H37 B9 P3 Rh S
• Calculated formula: C9 H36.917 B9 P3 Rh S
• Title of publication: Chemistry of 11-vertex rhodathiaboranes: reactions with monodentate phosphines.
• Authors of publication: Calvo, Beatriz; Kess, Martin; Macías, Ramón; Cunchillos, Carmen; Lahoz, Fernando J.; Kennedy, John D.; Oro, Luis A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 24
• Pages of publication: 6555 - 6564
• a: 16.306 ± 0.001 Å
• b: 15.579 ± 0.001 Å
• c: 17.484 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4441.5 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0264
• Residual factor for significantly intense reflections: 0.0252
• Weighted residual factors for significantly intense reflections: 0.0684
• Weighted residual factors for all reflections included in the refinement: 0.0693
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7378 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No