Crystallography Open Database

Information card for entry 7016186

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Coordinates	7016186.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H34 N3 Si1.5 Sm
Calculated formula	C23 H34 N3 Si1.5 Sm
Title of publication	Cubic and doubly-fused cubic samarium clusters from Sm(ii)-mediated reduction of organic azides and azobenzenes.
Authors of publication	Pan, Cheng-Ling; Chen, Wan; Su, Shengqun; Pan, Yu-Song; Wang, Jing
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	31
Pages of publication	7941 - 7945
a	22.1973 ± 0.0005 Å
b	22.1973 ± 0.0005 Å
c	20.2578 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	9981.4 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	5
Space group number	88
Hermann-Mauguin space group symbol	I 41/a :2
Hall space group symbol	-I 4ad
Residual factor for all reflections	0.0659
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0838
Weighted residual factors for all reflections included in the refinement	0.1058
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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