Information card for entry 7016265

Structure parameters

• Common name: HB(C3H3N2)3Zr(N(CH3)2)2NH2B(C6F5)3, c6 H14
• Formula: C37 H38 B2 F15 N9 Zr
• Calculated formula: C37 H24 B2 F15 N9 Zr
• Title of publication: Tris(pyrazolyl)borate amidoborane complexes of the group 4 metals.
• Authors of publication: Fuller, Anna-Marie; Hughes, David L.; Lancaster, Simon J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 28
• Pages of publication: 7434 - 7441
• a: 12.696 ± 0.0004 Å
• b: 24.1645 ± 0.0008 Å
• c: 14.1775 ± 0.0005 Å
• α: 90°
• β: 105.824 ± 0.003°
• γ: 90°
• Cell volume: 4184.7 ± 0.2 ų
• Cell temperature: 140 ± 1 K
• Ambient diffraction temperature: 140 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0818
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.0987
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No