Interaction of Co(ii), Ni(ii) and Cu(ii) with dibenzo-substituted macrocyclic ligands incorporating both symmetrically and unsymmetrically arranged N, O and S donors.
Authors of publication
Vasilescu, I. M.; Baldwin, D. S.; Bourne, D. J.; Clegg, J. K.; Li, F.; Lindoy, L. F.; Meehan, G. V.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
34
Pages of publication
8675 - 8684
a
9.1852 ± 0.001 Å
b
10.0015 ± 0.0009 Å
c
10.9234 ± 0.0008 Å
α
71.742 ± 0.006°
β
86.09 ± 0.007°
γ
73.961 ± 0.008°
Cell volume
915.69 ± 0.15 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0868
Residual factor for significantly intense reflections
0.0604
Weighted residual factors for significantly intense reflections
0.1555
Weighted residual factors for all reflections included in the refinement
0.173
Goodness-of-fit parameter for all reflections included in the refinement
