Information card for entry 7016519

Structure parameters

• Formula: C52.5 H34 Cl1.5 Co F24 N4.5 Ni O9 S6
• Calculated formula: C52 H33.5 Co F24 N4.5 Ni O9 S6
• Title of publication: Exploratory studies on coordination chemistry of a redox-active bridging ligand: synthesis, properties and solid state structures of the complexes.
• Authors of publication: Ran, Ying-Fen; Liu, Shi-Xia; Sereda, Olha; Neels, Antonia; Decurtins, Silvio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 32
• Pages of publication: 8193 - 8198
• a: 16.3332 ± 0.0014 Å
• b: 17.221 ± 0.0017 Å
• c: 25.434 ± 0.002 Å
• α: 70.737 ± 0.007°
• β: 78.157 ± 0.007°
• γ: 70.913 ± 0.007°
• Cell volume: 6344 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1685
• Residual factor for significantly intense reflections: 0.0731
• Weighted residual factors for significantly intense reflections: 0.1628
• Weighted residual factors for all reflections included in the refinement: 0.1852
• Goodness-of-fit parameter for all reflections included in the refinement: 0.831
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No