Crystalline metal (Li, Mg, Ca, Sr, Ba, Sn, Pb) complexes of the new chelating N,N'-dianionic [1,2-N(R)C(6)H(4)(CH(2)NR)](2-) ligand (R = SiMe(3), CH(2)Bu(t)).
Authors of publication
Caro, Catherine F.; Coles, Martyn P.; Hitchcock, Peter B.; Lappert, Michael F.; Pierssens, Luc J.-M.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2011
Journal volume
40
Journal issue
38
Pages of publication
9821 - 9830
a
19.787 ± 0.007 Å
b
9.808 ± 0.003 Å
c
21.951 ± 0.009 Å
α
90 ± 0.03°
β
99.7 ± 0.03°
γ
90 ± 0.02°
Cell volume
4199 ± 3 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0855
Residual factor for significantly intense reflections
0.0556
Weighted residual factors for significantly intense reflections
0.1322
Weighted residual factors for all reflections included in the refinement
0.15
Goodness-of-fit parameter for all reflections included in the refinement
