Information card for entry 7016700

Structure parameters

• Formula: C68 H84 Cl16 N6 P2 Pd2 Ru2
• Calculated formula: C68 H84 Cl16 N6 P2 Pd2 Ru2
• Title of publication: The use of 1,2-dipiperidinoacetylene for the preparation of monometallic diaminoacetylene and homo- or heterobimetallic diaminodicarbene ruthenium(ii) complexes.
• Authors of publication: Petrov, Alex R.; Bannenberg, Thomas; Daniliuc, Constantin G.; Jones, Peter G.; Tamm, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 40
• Pages of publication: 10503 - 10512
• a: 17.1006 ± 0.0004 Å
• b: 18.8239 ± 0.0004 Å
• c: 21.009 ± 0.0006 Å
• α: 94.226 ± 0.002°
• β: 110.213 ± 0.002°
• γ: 98.865 ± 0.002°
• Cell volume: 6211.5 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0678
• Weighted residual factors for all reflections included in the refinement: 0.0702
• Goodness-of-fit parameter for all reflections included in the refinement: 0.892
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No